反应条件
1: 97 percent / NMP, 4 Angstroems MS, TPAP / CH2Cl2 / 1.5 h
2: 84 percent / p-TsOH*H2O / benzene / 8 h / Heating
3: 99 percent / TBAF / tetrahydrofuran / 1 h / Ambient temperature
4: 91 percent / TeCl4, 2,6-lutidine / CH2Cl2 / 1 h
5: 1.) TMSBr, 2.) HCl / 1.) CH2Cl2, rt, 2 h, 2.) H2O, 1 h
View Scheme
参考文献
Blagg, Brian S. J.; Poulter, C. Dale
Journal of Organic Chemistry, 1999 , vol. 64, # 5 p. 1508 - 1511
