1-丙基-2(1H)-吡啶酮合成路线 （共 12 条）
反应条件
nickel-copper T=180 - 237°C; P=29420.3 Torr; Hydrogenation.Anfangsdruck;
参考文献
Renault
Bulletin de la Societe Chimique de France, 1953 , p. 1001,1004
反应条件
chloro-trimethyl-silane; lithium hexamethyldisilazane in acetonitrile
T=50°C; Hilbert-Johnson reaction; P=4500450000 Torr; 96 h; Microwave irradiation;
参考文献
Iida, Hirokazu; Suda, Machiko; Nakajima, Etsuko; Hakamatsuka, Hiroko; Nagashima, Yuka; Joho, Kouta; Amemiya, Kenta; Moromizato, Tatsuya; Matsumoto, Kiyoshi; Murakami, Yasuoki; Hamana, Hiroshi
Heterocycles, 2010 , vol. 81, # 9 p. 2057 - 2062
反应条件
K3Fe(CN)6; potassium hydroxide in benzine; water
T=20°C; 2 h;
参考文献
Yu, Yang; Zhu, Chenggen; Wang, Sujuan; Song, Weixia; Yang, Yongchun; Shi, Jiangong
Journal of Natural Products, 2013 , vol. 76, # 12 p. 2226 - 2233
反应条件
T=150°C; Hilbert-Johnson reaction; 0.0833333 h; Microwave irradiation;
参考文献
Iida, Hirokazu; Suda, Machiko; Nakajima, Etsuko; Hakamatsuka, Hiroko; Nagashima, Yuka; Joho, Kouta; Amemiya, Kenta; Moromizato, Tatsuya; Matsumoto, Kiyoshi; Murakami, Yasuoki; Hamana, Hiroshi
Heterocycles, 2010 , vol. 81, # 9 p. 2057 - 2062
反应条件
1: N,N-dimethyl-formamide / 12 h / 20 °C
2: potassium hydroxide; K3Fe(CN)6 / water; benzine / 2 h / 20 °C
View Scheme
参考文献
Yu, Yang; Zhu, Chenggen; Wang, Sujuan; Song, Weixia; Yang, Yongchun; Shi, Jiangong
Journal of Natural Products, 2013 , vol. 76, # 12 p. 2226 - 2233
反应条件
ethanol; nickel
Hydrogenation;
参考文献
Michant'ew et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1874;engl.Ausg.S.1844
反应条件
1: sodium hydride
2: 0.08 h / Microwave irradiation
View Scheme
参考文献
Iida, Hirokazu; Suda, Machiko; Nakajima, Etsuko; Hakamatsuka, Hiroko; Nagashima, Yuka; Joho, Kouta; Amemiya, Kenta; Moromizato, Tatsuya; Matsumoto, Kiyoshi; Murakami, Yasuoki; Hamana, Hiroshi
Heterocycles, 2010 , vol. 81, # 9 p. 2057 - 2062
反应条件
1: sodium hydride
2: 0.08 h / 150 °C / Microwave irradiation
View Scheme
参考文献
Iida, Hirokazu; Suda, Machiko; Nakajima, Etsuko; Hakamatsuka, Hiroko; Nagashima, Yuka; Joho, Kouta; Amemiya, Kenta; Moromizato, Tatsuya; Matsumoto, Kiyoshi; Murakami, Yasuoki; Hamana, Hiroshi
Heterocycles, 2010 , vol. 81, # 9 p. 2057 - 2062
参考文献
Raeth
Justus Liebigs Annalen der Chemie, 1931 , vol. 489, p. 107,117
反应条件
Hilbert-Johnson reaction; 0.0833333 h; Microwave irradiation;
参考文献
Iida, Hirokazu; Suda, Machiko; Nakajima, Etsuko; Hakamatsuka, Hiroko; Nagashima, Yuka; Joho, Kouta; Amemiya, Kenta; Moromizato, Tatsuya; Matsumoto, Kiyoshi; Murakami, Yasuoki; Hamana, Hiroshi
Heterocycles, 2010 , vol. 81, # 9 p. 2057 - 2062
