4-甲基伞形酮酰-Β-D-吡喃葡糖酸苷合成路线 （共 20 条）
反应条件
methanol; sodium methylate T=20°C; 0.5 h;
参考文献
Touisni, Nadia; Maresca, Alfonso; McDonald, Paul C.; Lou, Yuanmei; Scozzafava, Andrea; Dedhar, Shoukat; Winum, Jean-Yves; Supuran, Claudiu T.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 24 p. 8271 - 8277
反应条件
1: 43 percent / aq. NaOH / acetone / 7 h / Ambient temperature 2: 6mM methanolic MeONa / 5 h / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 274, p. 285 - 302
反应条件
1: 43 percent / aq. NaOH / acetone / 7 h / Ambient temperature 2: 6mM methanolic MeONa / 5 h / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 274, p. 285 - 302
反应条件
1: HBr / acetic acid / Ambient temperature 2: 43 percent / aq. NaOH / acetone / 7 h / Ambient temperature 3: 6mM methanolic MeONa / 5 h / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 274, p. 285 - 302
反应条件
1.1: morpholine / dichloromethane / 20 °C / Inert atmosphere 2.1: dichloromethane / 1 h / 0 °C / Inert atmosphere 2.2: 0.5 h / 0 °C / Inert atmosphere 3.1: boron trifluoride dimethyl etherate / dichloromethane / 20 °C / Inert atmosphere 4.1: methanol; sodium methylate / 0.5 h / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 24 p. 8271 - 8277
反应条件
1.1: dichloromethane / 1 h / 0 °C / Inert atmosphere 1.2: 0.5 h / 0 °C / Inert atmosphere 2.1: boron trifluoride dimethyl etherate / dichloromethane / 20 °C / Inert atmosphere 3.1: methanol; sodium methylate / 0.5 h / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 24 p. 8271 - 8277
反应条件
1: boron trifluoride dimethyl etherate / dichloromethane / 20 °C / Inert atmosphere 2: methanol; sodium methylate / 0.5 h / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 24 p. 8271 - 8277
反应条件
β-1,3-1,4-D-glucanase from Rhodothermus marinus in acetate buffer T=37°C; pH=4.0; Enzyme kinetics;
参考文献
Carbohydrate Research, , vol. 338, # 14 p. 1455 - 1467
反应条件
β-1,3-1,4-D-glucanase from Rhodothermus marinus in acetate buffer T=37°C; pH=4.0; Enzyme kinetics;
参考文献
Carbohydrate Research, , vol. 338, # 14 p. 1455 - 1467
反应条件
magnesium chloride T=37°C; pH=7.5; 0.25 h; aq. phosphate bufferEnzymatic reaction; Kinetics; Concentration;
参考文献
Molecular Pharmacology, , vol. 79, # 3 p. 472 - 478
