palladium diacetate; tetrabutylammomium bromide; potassium carbonate in water T=25°C; 16 h;
参考文献
Jung, Michael E.; Ku, Jin-Mo; Du, Liutao; Hu, Hailiang; Gatti, Richard A.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 19 p. 5842 - 5848
Novikov, V. N.; Polyakov, V. E.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 6 p. 563 - 566
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 6 p. 747 - 750
1: 88 percent / benzyltrimethylammonium bromide; Pd(OAc)2; aq. K2CO3 / 3 h 2: 99 percent / LiAlH4 / diethyl ether / 1 h / 0 °C View Scheme
参考文献
Jung, Michael E.; Ku, Jin-Mo; Du, Liutao; Hu, Hailiang; Gatti, Richard A.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 19 p. 5842 - 5848
1: piperidine; 5-bromo-2-furancarboxaldehyde With triethylamine in 1,4-dioxane; water 4 h; Heating; 2: N-phenyl-maleimide With magnesium sulfate in 1,4-dioxane; water Diels-Alder reaction; 18 h; Heating; Further stages.;
lithium aluminium tetrahydride in diethyl ether T=0°C; 2 h;
参考文献
Martin-Matute, Belen; Nevado, Cristina; Cardenas, Diego J.; Echavarren, Antonio M.
Journal of the American Chemical Society, 2003 , vol. 125, # 19 p. 5757 - 5766