1,3,4,6-四-氧-乙酰-Β-D-吡啶甘露糖合成路线 （共 20 条）
反应条件
hydrogenchloride in acetone T=20°C; 0.0833333 h;
参考文献
Pozsgay; Glaudemans; Robbins; Schneerson
Tetrahedron, 1992 , vol. 48, # 47 p. 10249 - 10264
反应条件
trifluoroacetic acid in water; acetonitrile T=0°C;
参考文献
US2006/67888 A1, ;
Page/Page column 11; sheet 7 ;
反应条件
ethanol; trimethylamine; benzene
参考文献
Chemische Berichte, , vol. 63, p. 386,390
反应条件
hydrogen; platinum(IV) oxide in ethyl acetate 48 h;
参考文献
Lichtenthaler, Frieder W.; Jarglis, Pan
Chemische Berichte, 1980 , vol. 113, # 2 p. 489 - 510
反应条件
trifluoroacetic acid in acetonitrile T=0°C; 3 h; Yields of byproduct given;
参考文献
Franzyk, Henrik; Meldal, Morten; Paulsen, Hans; Bock, Klaus
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 22 p. 2883 - 2898
反应条件
1: 14 percent / Cl2, Ag2CO3 / diethyl ether; H2O / 1.) 20 min ice-cooling, 2.) 30 min, room temp. 2: 19 percent / H2 / PtO2 / ethyl acetate / 48 h View Scheme
参考文献
Chemische Berichte, , vol. 113, # 2 p. 489 - 510
反应条件
1: 60 percent / RuO4 / CCl4; CH2Cl2 / 2 h / Ambient temperature 2: 19 percent / H2 / PtO2 / ethyl acetate / 48 h View Scheme
参考文献
Chemische Berichte, , vol. 113, # 2 p. 489 - 510
反应条件
1: 1) glacial AcOH, Ac2O, 30percent HBr/AcOH, 2) 2,4,6-trimethylpyridine / 1) 0 deg C to r.t., 4 h, 2) 14 h, r.t. 2: 32.4 percent / 1N aq. HCl / acetone / 0.08 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 48, # 47 p. 10249 - 10264
反应条件
sodium acetate in water T=20 - 30°C;
参考文献
Sasaki, Eita; Ogasawara, Yasushi; Liu, Hung-Wen
Journal of the American Chemical Society, 2010 , vol. 132, # 21 p. 7405 - 7417
反应条件
phosphorus tribromide
参考文献
Kovac
Carbohydrate research, 1986 , vol. 153, # 1 p. 168 - 170
