[2,2-二(三甲基硅烷基)乙烯基](三甲基)硅烷合成路线 （共 15 条）
反应条件
methyl-magnesium iodide; lithium tetrachloromanganate(II) in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=0°C; 3 h;
参考文献
Hibino, Jun-ichi; Nakatsukasa, Shigeki; Fugami, Keigo; Matsubara, Seijiro; Oshima, Koichiro; Nozaki, Hitosi
Journal of the American Chemical Society, 1985 , vol. 107, # 22 p. 6416 - 6417
反应条件
CoCl2 in tetrahydrofuran; diethyl ether
T=-20°C;
参考文献
Ohmiya, Hirohisa; Yorimitsu, Hideki; Oshima, Koichiro
Angewandte Chemie - International Edition, 2005 , vol. 44, # 22 p. 3488 - 3490
反应条件
Au nanoparticles/TiO2 (1 mol percent) in 1,2-dichloro-ethane
T=65°C; 2 h; stereoselective reaction;
参考文献
Gryparis, Charis; Kidonakis, Marios; Stratakis, Manolis
Organic Letters, 2013 , vol. 15, # 23 p. 6038 - 6041
参考文献
Okazaki,R.; Ishii,A.; Inamoto,N.
Journal of the American Chemical Society, 1987 , vol. 109, p. 279
反应条件
dihydrogen hexachloroplatinate in isopropyl alcohol
T=120 - 130°C; 47 h;
参考文献
Sheludyakov, V. D.; Korshunov, A. I.; Lakhtin, V. G.; Timofeev, V. S.; Slyusarenko, T. F.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 12 p. 2743 - 2750,2429 - 2435
反应条件
platinum(0)-methyldivinyldisiloxane
T=90°C; P=760 Torr; 21 h;
参考文献
Suzuki, Toshio; Lo, Peter Y.
Journal of Organometallic Chemistry, 1990 , vol. 396, # 2/3 p. 299 - 305
反应条件
in benzene
T=5°C; 17 h; Irradiationphotolysis;
参考文献
Okazaki,R.; Ishii,A.; Inamoto,N.
Journal of the American Chemical Society, 1987 , vol. 109, p. 279
反应条件
in toluene
4 h; Heating;
参考文献
Muccioli, Adriano B.; Simpkins, Nigel S.; Mortlock, Andrew
Journal of Organic Chemistry, 1994 , vol. 59, # 18 p. 5141 - 5143
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Dishington, Allan P.; Douthwaite, Richard E.; Mortlock, Andrew; Muccioli, Adriano B.; Simpkins, Nigel S.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 3 p. 323 - 337
参考文献
Okazaki,R.; Ishii,A.; Inamoto,N.
Journal of the American Chemical Society, 1987 , vol. 109, p. 279
反应条件
platinum(0)-tetramethyldivinyldisiloxane
T=90°C; P=760 Torr; 24 h; other disilylethynes, var. times, temp. and pressures; Product distributionMechanism;
参考文献
Suzuki, Toshio; Lo, Peter Y.
Journal of Organometallic Chemistry, 1990 , vol. 396, # 2/3 p. 299 - 305
