4-(三氟甲基)苯甲酰胺合成路线 （共 35 条）
反应条件
ammonium hydroxide in water T=20°C; 3.75 h;
参考文献
Reuman, Michael; Hu, Zhiyong; Kuo, Gee-Hong; Li, Xun; Russell, Ronald K.; Shen, Lan; Youells, Scott; Zhang, Yongzheng
Organic Process Research and Development, 2007 , vol. 11, # 6 p. 1010 - 1014
反应条件
tris-(dibenzylideneacetone)dipalladium(0); {(S)-1-[(R)-(diphenylphosphino)ferrocenyl]}ethyl-di-tert-butylphosphine; ammonium carbamate; sodium hydrogencarbonate in 1,4-dioxane T=100°C; 20 h; Inert atmosphere;
参考文献
Nielsen, Dennis U.; Taaning, Rolf H.; Lindhardt, Anders T.; Gogsig, Thomas M.; Skrydstrup, Troels
Organic Letters, 2011 , vol. 13, # 16 p. 4454 - 4457
反应条件
Wilkinson's catalyst; acetaldehyde oxime in toluene T=110°C;
参考文献
Kang, Dahye; Lee, Jinwoo; Lee, Hee-Yoon
Organic Syntheses, 2012 , vol. 89, p. 66 - 72
反应条件
tert.-butylhydroperoxide; ammonium hydroxide in water T=100°C; 16 h;
参考文献
Wu, Xiao-Feng; Sharif, Muhammad; Feng, Jian-Bo; Neumann, Helfried; Pews-Davtyan, Anahit; Langer, Peter; Beller, Matthias
Green Chemistry, 2013 , vol. 15, # 7 p. 1956 - 1961
反应条件
tert.-butylhydroperoxide; ammonium hydroxide in water T=80°C; 12 h;
参考文献
Wang, Liang; Shen, Chen; Wang, Hai-Ping; Zhou, Wei-You; Sun, Fu-An; He, Ming-Yang; Chen, Qun
Journal of Chemical Research, 2012 , vol. 36, # 8 p. 460 - 462
反应条件
Rh(cod)(IMes)Cl; p-(trifluoromethyl)-benzonitrile; toluene-4-sulfonic acid in toluene T=80°C; 6 h;
参考文献
Kim, Min; Lee, Jinwoo; Lee, Hee-Yoon; Chang, Sukbok
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 1807 - 1812
反应条件
hydroxylamine hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); [(t-Bu)3PH]BF4 in 1,4-dioxane T=110°C; 0.333333 h; microwave irradiation;
参考文献
Wu, Xiongyu; Wannberg, Johan; Larhed, Mats
Tetrahedron, 2006 , vol. 62, # 19 p. 4665 - 4670
反应条件
hydroxylamine hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); [(t-Bu)3PH]BF4 in 1,4-dioxane T=150°C; 0.333333 h; microwave irradiation;
参考文献
Wu, Xiongyu; Wannberg, Johan; Larhed, Mats
Tetrahedron, 2006 , vol. 62, # 19 p. 4665 - 4670
反应条件
hydroxylamine hydrochloride; zinc trifluoromethanesulfonate in toluene T=100°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 53, # 7 p. 882 - 885
反应条件
1: With Y[N(Si(methyl)3)2]3(μ-Cl)Li(tetrahydrofuran)3 in dichloromethane T=20°C; 48 h; 2: With hydrogenchloride
参考文献
Journal of Organic Chemistry, , vol. 71, # 8 p. 3149 - 3153
