反应条件
in hydrogen fluoride
dry HF condensed at -196°C onto mixt. of ClF6AsF6 and CsBF4, warmed for 30 min to 25°C with stirring; cooled to -78°C, filtered under N2 (2 atm), volatile at 25°C pumped off for 1.5 h, sepd. by fractional condensation through series of traps kept at -112, -142, and -196°C; IR, Raman anal.;
参考文献
Christe, Karl O.; Wilson, William W.
Inorganic Chemistry, 1983 , vol. 22, p. 1950 - 1951
