1-(苯磺酰基)-1H-吡咯并[2,3-b]吡啶-2-甲醛合成路线 (共 2 条)
反应条件
water; potassium hydroxide in methanol T=20°C; 0.5 h; Inert atmosphere;
参考文献
GLAXO GROUP LIMITED; ATKINSON, Stephen John; BARKER, Michael David; CAMPBELL, Matthew; DIALLO, Hawa; DOUAULT, Clement; GARTON, Neil Stuart; LIDDLE, John; SHEPPARD, Robert John; WALKER, Ann, Louise; WELLAWAY, Christopher; WILSON, David Matthew
Patent: WO2014/15905 A1, 2014 ;
Location in patent: Page/Page column 47 ;
反应条件
sodium chlorite; sodium dihydrogenphosphate in tert-butyl benzene; 2-methyl-butane 3.16667 h;
参考文献
WO2006/50976 A1, ;
Page/Page column 30 ;
WO 2006/050976 A1