2,3-二甲基-2,3-二苯基丁烷合成路线 (共 146 条)
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran Heating;
参考文献
Bors, Daniel A.; Kaufman, Michael J.; Streitwieser, Andrew Jr.
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 6975 - 6982
反应条件
Ti(III)-citrate; Tris buffer; tetra(n-butyl)ammonium hydroxide; B12 in ethanol pH=8;
参考文献
Journal of Organic Chemistry, , vol. 67, # 3 p. 837 - 846
反应条件
magnesium in diethyl ether
参考文献
Popielarz; Arnold
Journal of the American Chemical Society, 1990 , vol. 112, # 8 p. 3068 - 3082
反应条件
t-BuON=NOt-Bu T=80°C; 0.5 h;
参考文献
Protasiewicz, J.; Mendenhall, G. D.
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3220 - 3222
反应条件
1: dimethyl zinc With VCl4 in tetrahydrofuran; hexane T=0°C; complexation; 0.5 h; 2: acetophenone in tetrahydrofuran; hexane Methylation; dimerization; 12 h; Heating;
参考文献
Kataoka, Yasutaka; Makihira, Isamu; Utsunomiya, Masaru; Tani, Kazuhide
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8540 - 8543
反应条件
[Co(PPh3)3Cl] in benzene 2 h; Ambient temperature;
参考文献
Yamada, Yasuji; Momose, Den-ichi
Chemistry Letters, 1981 , p. 1277 - 1278
Title/Abstract Full Text Show Details
Momose, Den-ichi; Iguchi, Kazuo; Sugiyama, Toshikazu; Yamada, Yasuji
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 5 p. 1840 - 1853
反应条件
sodium tetrahydroborate; (5,10,15,20-tetramesitylporphyrin)MnCl; oxygen in ethanol; benzene 0.583333 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 67, # 6 p. 1726 - 1733
反应条件
copper(l) iodide; chloro-trimethyl-silane; iodine; lanthanum in acetonitrile T=82°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 43, # 20 p. 3689 - 3691
反应条件
1: 95 percent / diethyl ether; hexane / 1.5 h / 20 °C 2: 90 percent / aq. NaOH; NaOCl / 20 °C 3: Thermolysis View Scheme
参考文献
Journal of the American Chemical Society, , vol. 123, # 16 p. 3706 - 3715
反应条件
dinitrogen monoxide; sodium tetrahydroborate; 5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride; tetreamethyl ammonium hydroxide in methanol; toluene 14 h; Reagent/catalystTime;
参考文献
Saito, Shunsuke; Ohtake, Hiro; Umezawa, Naoki; Kobayashi, Yuko; Kato, Nobuki; Hirobe, Masaaki; Higuchi, Tsunehiko
Chemical Communications, 2013 , vol. 49, # 79 p. 8979 - 8981