1,5-己二烯二环氧化物合成路线 (共 11 条)
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
参考文献
Lee, Sang Hyup; Kohn, Harold
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 3 p. 471 - 482
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform T=20°C; 24 h;
参考文献
De March, Pedro; Figueredo, Marta; Font, Josep; Raya, Javier; Alvarez-Larena, Angel; Piniella, Juan F.
Journal of Organic Chemistry, 2003 , vol. 68, # 6 p. 2437 - 2447
反应条件
dihydrogen peroxide in methanol; water T=64.84°C; 2 h; regioselective reaction;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 328, # 1-2 p. 60 - 67
反应条件
ethanol; silver(I) acetate
参考文献
Journal of the Chemical Society, , p. 1566,1572
反应条件
diethyl ether; sodium 1.2;5.6-dioxido-hexan(?) of boiling point 153 degree;
参考文献
Annales de Chimie (Cachan, France), , vol. <6> 22, p. 441,447
参考文献
Journal of the Chemical Society, , p. 3131,3133
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 1 h;
参考文献
Li, Xiaoyong; Burrell, Carmin E.; Staples, Richard J.; Borhan, Babak
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9026 - 9029
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Wiggins; Wood
Journal of the Chemical Society, 1950 , p. 1566,1572
参考文献
Wiggins; Wood
Journal of the Chemical Society, 1950 , p. 1566,1572
反应条件
1: trimethyl-sulfonium iodide With n-butyllithium in tetrahydrofuran; hexane
T=-10°C; 0.5 h;
2: 1,2-di(oxiran-2-yl)ethane in tetrahydrofuran; hexane
T=-10 - 20°C;
参考文献
UNIVERSITY OF KANSAS; BLAGG, Brian, S. J.; KUSUMA, Bhaskar, Reddy; SUNDSTROM, Teather
Patent: WO2013/119985 A1, 2013 ;
Location in patent: Paragraph 00352; 00353 ;