2-氨基-6-甲基苯甲酰胺合成路线 (共 3 条)
反应条件
hydrogen; palladium 10 on activated carbon in methanol P=2585.81 Torr; 1.5 h;
参考文献
Ahmad, Saleem; Ngu, Khehyong
Patent: US2006/178386 A1, 2006 ;
Location in patent: Page/Page column 15 ;
US 20060178386 A1
反应条件
1: in tetrahydrofuran T=50°C; 15 h; 2: With ammonia in tetrahydrofuran; water T=60°C; 3 h;
参考文献
Takeda Pharmaceutical Company Limited
Patent: EP1953148 A1, 2008 ;
Location in patent: Page/Page column 132 ;
EP 1953148 A1
反应条件
potassium hydroxide in ethanol RefluxInert atmosphere;
参考文献
Cheng, Xu; Vellalath, Sreekumar; Goddard, Richard; List, Benjamin
Journal of the American Chemical Society, 2008 , vol. 130, # 47 p. 15786 - 15787