苯并(1,2,3-cd:4,5,6-c'd')二苝合成路线 (共 3 条)
反应条件
trifluorormethanesulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; Scholl Reaction; 24 h; Inert atmosphereReflux;
参考文献
Thamatam, Rajesh; Skraba, Sarah L.; Johnson, Richard P.
Chemical Communications, 2013 , vol. 49, # 80 p. 9122 - 9124
反应条件
trifluorormethanesulfonic acid; oxygen in chlorobenzene Scholl Reaction; P=760.051 Torr; 24 h; Reflux;
参考文献
Thamatam, Rajesh; Skraba, Sarah L.; Johnson, Richard P.
Chemical Communications, 2013 , vol. 49, # 80 p. 9122 - 9124
反应条件
aluminium trichloride; sodium chloride T=130°C; 0.25 h;
参考文献
Bohnen, Angelika; Koch, Karl-Heinz; Luettke, Wolfgang; Muellen, Klaus
Angewandte Chemie, 1990 , vol. 102, # 5 p. 548 - 550