反应条件
1: 3-iodo-pyridine With copper(l) iodide; potassium carbonate; sulfur in N,N-dimethyl-formamide
T=90°C; Inert atmosphere;
2: With sodium tetrahydroborate in N,N-dimethyl-formamide
T=40°C; Inert atmosphereCooling with ice;
3: methyl iodide in N,N-dimethyl-formamide
T=20°C; Inert atmosphere;
参考文献
Jiang, Yongwen; Qin, Yuxia; Xie, Siwei; Zhang, Xiaojing; Dong, Jinhua; Ma, Dawei
Organic Letters, 2009 , vol. 11, # 22 p. 5250 - 5253
