反应条件
1: sodium periodate; silica gel / dichloromethane; water / 3.58 h 2: (S)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; chloroacetic acid / dimethyl sulfoxide / 20 °C 3: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 70 °C / Inert atmosphere 4: acetic acid; zinc / 34 h / 20 °C / Inert atmosphere View Scheme
参考文献
Rehak, Juraj; Huka, Martin; Latika, Attila; Brath, Henrich; Almassy, Ambroz; Hajzer, Viktoria; Durmis, Julius; Toma, Stefan; Sebesta, Radovan
Synthesis (Germany), 2012 , vol. 44, # 15 p. 2424 - 2430
