反应条件
in benzene stirring for 3 days under N2-atmosphere, filtering off an off-white ppt. (probably a polymeric organotin compound), adding 1 N HCl, stirring (few minutes), evaporating the benzene layer gave {IrBr(COD)}2, water layer afforded the ammonium salt; identification: (1)H-NMR, FD mass spectroscopy;
参考文献
Zeijden, Adolphus A. H. van der; Koten, Gerard van; Wouters, Jacqueline M. A.; Wijsmuller, Willem F. A.; Grove, David M.; et al.
Journal of the American Chemical Society, 1988 , vol. 110, # 16 p. 5354 - 5361