(2,6-二甲基苯基)苯甲酸酯合成路线 (共 5 条)
反应条件
tetrabutyl-ammonium chloride; sodium hydroxide in dichloromethane; water T=0°C; 0.0833333 h;
参考文献
Simion, Alina Marieta; Hashimoto, Iwao; Mitoma, Yoshiharu; Egashira, Naoyoshi; Simion, Cristian
Synthetic Communications, 2012 , vol. 42, # 6 p. 921 - 931
反应条件
p-NO2-benzoic anhydride; scandium tris(trifluoromethanesulfonate) in nitromethane; acetonitrile 1 h; Ambient temperature;
参考文献
Ishihara, Kazuaki; Kubota, Manabu; Kurihara, Hideki; Yamamoto, Hisashi
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4560 - 4567
反应条件
in not given byproducts: C6H5CH3, 2,6-(CH3)2C6H3OH, C6H5COOCH2-2,6-(CH3)2C6H3;
参考文献
Khoo; Lee
Tetrahedron, 1970 , vol. 26, p. 4261,4265, 4266, 4277
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.6, page 61 - 62
反应条件
in not given byproducts: C6H5CH3, 2,6-(CH3)2C6H3OH, C6H5COOCH2-2,6-(CH3)2C6H3;
参考文献
Khoo; Lee
Tetrahedron, 1970 , vol. 26, p. 4261,4265, 4266, 4277
Full Text View citing articles Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.6, page 61 - 62
反应条件
aluminium trichloride
T=130 - 140°C;
参考文献
Fujio,M. et al.
Bulletin of the Chemical Society of Japan, 1975 , vol. 48, p. 2127 - 2133