反应条件
1: 1.) 2-chloro-4,6-dimethoxy-1,3,5-triazine,N-methylmorpholine; 2) N-methylmorpholine / 1) CH2Cl2, 0-5 deg C, 2 h; 2) CH2Cl2, 0 deg C, 2 h, rt, 20-24 h 2: LiI / ethyl acetate / Heating 3: 59 percent / Ac2O / 1) 60-80 deg C, 45 min; 2) 120-125 deg C, 2-3 h View Scheme
参考文献
Nayyar, Naresh K.; Hutchison, Darrell R.; Martinelli, Michael J.
Journal of Organic Chemistry, 1997 , vol. 62, # 4 p. 982 - 991
