1,3,5-三氯-2-硝基苯合成路线 （共 24 条）
反应条件
tert.-butylhydroperoxide; 3 A molecular sieve; zirconium tetra-t-butoxide in dichloromethane 48 h; Heating;
参考文献
Krohn, Karsten; Kuepke, Jochen; Rieger, Hagen
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 4 p. 335 - 339
参考文献
Journal of the American Chemical Society, , vol. 62, p. 511,512
Journal of the Chemical Society, , p. 1525,1527
反应条件
in acetone T=22°C; 10 h;
参考文献
Murray, Robert W.; Rajadhyaksha, Shirish N.; Mohan, Lily
Journal of Organic Chemistry, 1989 , vol. 54, # 24 p. 5783 - 5788
反应条件
1: calcium hypochlorite / >40 View Scheme
参考文献
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, , vol. <5> 18 I, p. 100
参考文献
Journal of the American Chemical Society, , vol. 62, p. 511,512
Justus Liebigs Annalen der Chemie, , vol. 192, p. 230
American Chemical Journal, , vol. 9, p. 354
参考文献
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, , vol. <5> 18 I, p. 100
反应条件
potassium fluoride; dimethyl sulfoxide T=180°C;
参考文献
Shaw,G.C.; Seaton,D.L.
Journal of Organic Chemistry, 1961 , vol. 26, p. 5227 - 5228
反应条件
1: methanol / 150 °C 2: acetic acid anhydride; nitric acid View Scheme
参考文献
Hodgson; Batty
Journal of the Chemical Society, 1934 , p. 1433
反应条件
1: 100.6 percent / nitric acid / H2SO4 / 25 - 75 °C 2: nitric acid / various solvent(s) / 150 °C / acidity dependence of formation of TetCDNB View Scheme
参考文献
Moodie, Roy B.; Payne, Malcolm A.; Schofield, Kenneth
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1457 - 1464
反应条件
hydrazine hydrate in dimethyl sulfoxide 6 h; Heating;
参考文献
Stepanov, P. A.; Yurchenko, G. A.
J. Appl. Chem. USSR (Engl. Transl.), 1991 , vol. 64, # 12 p. 2703 - 2704,2530 - 2531
