3,5-二[3,5-二(甲氧羰基)苯氧甲基]苯酚合成路线 （共 7 条）
反应条件
hydrogenchloride in tetrahydrofuran; water; isopropyl alcohol
T=20°C; Cooling with iceInert atmosphere;
参考文献
Feng, Yu; Liu, Zi-Tong; Liu, Ji; He, Yan-Mei; Zheng, Qi-Yu; Fan, Qing-Hua
Journal of the American Chemical Society, 2009 , vol. 131, p. 7950 - 7951
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Hoeger, Sigurd
Synthesis, 1997 , # 1 p. 20 - 22
反应条件
sodium methylate in methanol; benzene
0.5 h; Heating;
参考文献
Krishna Maiti, Amiya; Martinez, Ricardo; Mestres, Ramon; Tortajada, Amparo; Villar, Felix
Tetrahedron, 2001 , vol. 57, # 16 p. 3397 - 3401
反应条件
1: 78 percent / DEAD, Ph3P / tetrahydrofuran / Ambient temperature
2: 87 percent / Bu4NF / tetrahydrofuran / 1 h / Ambient temperature
View Scheme
参考文献
Hoeger, Sigurd
Synthesis, 1997 , # 1 p. 20 - 22
反应条件
1: 36 percent / NBS; tert-butylperoxide / CCl4 / 24 h / Heating; illumination
2: 89 percent / K2CO3; 18-crown-6 / acetone / 24 h / Heating
3: 94 percent / sodium methoxide / benzene; methanol / 0.5 h / Heating
View Scheme
参考文献
Krishna Maiti, Amiya; Martinez, Ricardo; Mestres, Ramon; Tortajada, Amparo; Villar, Felix
Tetrahedron, 2001 , vol. 57, # 16 p. 3397 - 3401
反应条件
1: 73 percent / pyridine / 3 h / 20 °C
2: 36 percent / NBS; tert-butylperoxide / CCl4 / 24 h / Heating; illumination
3: 89 percent / K2CO3; 18-crown-6 / acetone / 24 h / Heating
4: 94 percent / sodium methoxide / benzene; methanol / 0.5 h / Heating
View Scheme
参考文献
Krishna Maiti, Amiya; Martinez, Ricardo; Mestres, Ramon; Tortajada, Amparo; Villar, Felix
Tetrahedron, 2001 , vol. 57, # 16 p. 3397 - 3401
反应条件
1: LiAlH4
2: PPh3, DEAD
3: TBAF
View Scheme
参考文献
Zafar, Abdullah; Yang, Ji; Geib, Steven J.; Hamilton, Andrew D.
Tetrahedron Letters, 1996 , vol. 37, # 14 p. 2327 - 2330
