3-苄氧基-4-甲氧苄醇合成路线 （共 20 条）
反应条件
sodium tetrahydroborate in ethanol; water T=20 - 25°C; 1 h;
参考文献
Bhandari, Prabha; Crombie, Leslie; Daniels, Peter; Holden, Ian; Bruggen, Nicholas Van; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 7 p. 839 - 850
反应条件
potassium tert-butylate in propan-1-ol T=60 - 90°C; 5.5 h; Heating / reflux;
参考文献
EURO-CELTIQUE S.A.
Patent: EP1202628 B1, 2004 ;
Location in patent: Page 11 ;
EP 1202628 B1
反应条件
1: 89 percent / NaHCO3; KI / acetonitrile / 10 h / Heating 2: 96 percent / NaBH4 / methanol / 2 h / 20 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 15, # 7 p. 1145 - 1149
反应条件
potassium carbonate in acetone 4 h; RefluxInert atmosphere;
参考文献
Taylor, Laura L.; Goldberg, Frederick W.; Hii, King Kuok Mimi
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 22 p. 4424 - 4432
反应条件
1: triphenylphosphine; diisopropyl azo-dicarboxylate / tetrahydrofuran / 0 °C 2: sodium borohydride / methanol View Scheme
参考文献
Organic Letters, , vol. 6, # 3 p. 397 - 400
反应条件
1: K2CO3 / dimethylformamide / 5 h / 40 - 50 °C 2: NaBH4, 0.5N aq. NaOH / tetrahydrofuran / 2.5 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 42, # 6 p. 1076 - 1087
反应条件
1: 89 percent / NaHCO3; KI / acetonitrile / 10 h / Heating 2: 96 percent / NaBH4 / methanol / 2 h / 20 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 15, # 7 p. 1145 - 1149
参考文献
Justus Liebigs Annalen der Chemie, , vol. 544, p. 30,58
参考文献
Justus Liebigs Annalen der Chemie, , vol. 544, p. 30,58
反应条件
1: 97 percent / SOCl2, pyridine / diethyl ether / 0.5 h / below 5 deg C 2: 92 percent / KI, urea / acetone / 6 h / Heating 3: H2 / 10percent Pd/C / acetone / 1 h / Ambient temperature 4: 10percent aq. NaOH / 1 h / 0 °C View Scheme
参考文献
Bhandari, Prabha; Crombie, Leslie; Daniels, Peter; Holden, Ian; Bruggen, Nicholas Van; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 7 p. 839 - 850
