4-苄氧基-3-甲氧基-beta-硝基苯乙烯合成路线 （共 10 条）
反应条件
ammonium acetate; acetic acid T=90°C; 4 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 15 p. 4862 - 4871
反应条件
1: KOH / ethanol / Heating 2: NH4OAc / acetic acid / Heating View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 1417 - 1423
反应条件
1.1: sodium hydride / tetrahydrofuran; mineral oil / 10 - 20 °C / Inert atmosphere 1.2: 18 h / Reflux; Inert atmosphere 2.1: ammonium acetate / acetic acid / 5 h / Inert atmosphere; Reflux View Scheme
参考文献
Arkivoc, , vol. 2011, # 5 p. 167 - 179
反应条件
1: KOH / ethanol / Heating 2: NH4OAc / acetic acid / Heating View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 1417 - 1423
反应条件
sodium acetate; acetic anhydride 0.0833333 h; Heating;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 2.2 p. 280 - 288
Zhurnal Organicheskoi Khimii, , vol. 28, # 2 p. 348 - 358
反应条件
ethanol; N-methylamine hydrochloride; sodium carbonate T=40 - 50°C;
参考文献
Scientific Papers of the Institute of Physical and Chemical Research (Japan), vol. 6, p. 154
Chem. Zentralbl., , vol. 99, # I p. 1027
反应条件
1: 71 percent / KOH, tetrabutylammonium bromide / ethanol / 1 h / 0 °C 2: 85 percent / AcONa. Ac2O / 0.08 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 2.2 p. 280 - 288
Zhurnal Organicheskoi Khimii, , vol. 28, # 2 p. 348 - 358
反应条件
1.1: LiAlH4 / diethyl ether / 30 h / Heating 1.2: 80 percent / NaOH / diethyl ether; H2O / 0.5 h / cooling 2.1: 100 percent / 12 h / 20 °C 3.1: 86 percent / POCl3 / toluene / 1 h / 85 °C View Scheme
参考文献
Reimann, Eberhard; Grasberger, Fritz
Monatshefte fur Chemie, 2005 , vol. 136, # 2 p. 193 - 209
反应条件
1: With lithium aluminium tetrahydride in diethyl ether 30 h; Heating; 2: With sodium hydroxide in diethyl ether; water 0.5 h; cooling;
参考文献
Reimann, Eberhard; Grasberger, Fritz
Monatshefte fur Chemie, 2005 , vol. 136, # 2 p. 193 - 209
反应条件
1.1: LiAlH4 / diethyl ether / 30 h / Heating
1.2: 80 percent / NaOH / diethyl ether; H2O / 0.5 h / cooling
2.1: 100 percent / 12 h / 20 °C
View Scheme
参考文献
Reimann, Eberhard; Grasberger, Fritz
Monatshefte fur Chemie, 2005 , vol. 136, # 2 p. 193 - 209
