2-氨基-5-甲基苯甲酸甲酯合成路线 (共 19 条)
反应条件
sulfuric acid 72 h; Reflux;
参考文献
Lawson, Christopher P. A. T.; Slawin, Alexandra M. Z.; Westwood, Nicholas J.
Chemical Communications, 2011 , vol. 47, # 3 p. 1057 - 1059
反应条件
hydrogenchloride; tin
参考文献
Journal of the Chemical Society, , p. 1513,1516
反应条件
sulfuric acid in methanol; water
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5128356 A1, 1992 ;
反应条件
in methanol; hexane; toluene T=20°C; 1 h;
参考文献
US2006/35908 A1, ;
Page/Page column 62 ;
US 20060035908 A1
反应条件
1: N-methyl-N-nitroso-p-toluene-sulphonamide With potassium hydroxide in diethyl ether; water 2: 2-amino-5-methyl-benzoic acid in diethyl ether 1 h;
参考文献
Schuler, Elisabeth; Juanico, Nacho; Teixido, Jordi; Michelotti, Enrique L.; Borrell, Jose I.
Heterocycles, 2006 , vol. 67, # 1 p. 161 - 173
反应条件
in diethyl ether 1 h; Inert atmosphere;
参考文献
Levesque, Patrick; Fournier, Pierre-Andre
Journal of Organic Chemistry, 2010 , vol. 75, # 20 p. 7033 - 7036
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>33, p. 58
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>33, p. 58
反应条件
1: aqueous hydrochloric acid; copper (II)-sulfate; water / Diazotization.Erhitzen des Reaktionsgemisches 2: aqueous hydrochloric acid View Scheme
参考文献
Hayashi
Journal of the Chemical Society, 1930 , p. 1513,1516
反应条件
in diethylene glycol dimethyl ether 0.191667 h; 225 deg C -> 185 deg C;
参考文献
Jones; Betteridge; Newell; Jackman
Journal of Heterocyclic Chemistry, 1989 , vol. 26, # 5 p. 1501 - 1507