1-甲基六氢-4H-氮杂卓-4-酮合成路线 （共 7 条）
反应条件
potassium hydroxide in ethanol T=5 - 10°C; 3 h; Yields of byproduct given;
参考文献
Polivka, Zdenek; Metys, Jan; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 9 p. 2034 - 2049
反应条件
potassium hydroxide in ethanol T=5 - 10°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 51, # 9 p. 2034 - 2049
反应条件
hydrogenchloride in methanol 1 h; Ambient temperature; Yield given;
参考文献
Synthetic Communications, , vol. 21, # 7 p. 881 - 884
反应条件
1: phosphate buffer, NaBH3CN / acetonitrile / 24 h / Ambient temperature 2: 10percent aq. HCl / methanol / 1 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 21, # 7 p. 881 - 884
反应条件
naphthalene; diethyl ether; lithium N-ethyl-N-phenylamide Erhitzen des Reaktionsprodukts mit wss. Schwefelsaeure.;
反应条件
1: 2.) NaBH4 / 1.) CH3OH, room temp. 2: 1.) 23percent aq. HCl, 2.) KOH / 1.) reflux, 3 h, 2.) methanol, reflux, 2 h View Scheme
参考文献
Scheffler; Engel; Kutscher; Sheldrick; Bell
Archiv der Pharmazie, 1988 , vol. 321, # 4 p. 205 - 208
参考文献
Levy, Jean; Laronze, Jean-Yves; Sapi, Janos
Tetrahedron Letters, 1988 , vol. 29, # 27 p. 3303 - 3306
