1,2-O-异亚丙基-D-呋喃葡萄糖合成路线 （共 73 条）
反应条件
pyridine; chloroform T=-15°C;
参考文献
Neal, Timothy R.; Schumann, William C.; Berridge, Marc S.; Landau, Bernard R.
Journal of Labelled Compounds and Radiopharmaceuticals, 2005 , vol. 48, # 11 p. 845 - 854
反应条件
1: 1,2-O-isopropylidene-α-D-glucofuranose With bis(tri-n-butyltin)oxide in toluene 2: benzoyl chloride
参考文献
Stick, Robert V.; Stubbs, Keith A.; Watts, Andrew G.
Australian Journal of Chemistry, 2004 , vol. 57, # 8 p. 779 - 786
反应条件
1: 1.) Bu2SnO / 1.) MeOH, reflux, 3 h, 2.) dioxane, from 5 deg C to 10 deg C, 1 h 2: 73 percent / pyridine 3: 14.2 percent / (Bu3Sn)2 / benzene / 4 h / 10 - 15 °C / Irradiation View Scheme
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
反应条件
iron(III) chloride in dichloromethane
参考文献
Wu, Qin-Pei; Zhou, Ming-Xin; Xi, Xiao-Dong; Song, Di; Wang, Yuan; Liu, Hai-Xia; Li, Yun-Zheng; Zhang, Qing-Shan
Tetrahedron Letters, 2008 , vol. 49, # 17 p. 2714 - 2718
反应条件
1: 1.) (Bu3Sn)2O, 2.) Br2 / 1.) CHCl3, heating
2: pyridine
3: 1.) TsNHNH2, 2.) NaBH4 / 1.) MeOH, 2.) MeOH, heating
4: CrO3 / pyridine; acetic anhydride
5: NaBH4 / ethanol
6: TBAF / tetrahydrofuran
View Scheme
参考文献
Robins; Guo; Wnuk
Journal of the American Chemical Society, 1997 , vol. 119, # 15 p. 3637 - 3638
反应条件
1: 91 percent / pyridine / 16 h / -15 °C
2: 92 percent / NaN3 / dimethylformamide / 20 h / 120 °C
3: 82 percent / aq. TFA / 0.5 h / 40 °C
View Scheme
参考文献
Fernandez, Jose M. Garcia; Mellet, Carmen Ortiz; Maciejewski, Sylwester; Defaye, Jacques
Journal of the Chemical Society, Chemical Communications, 1996 , # 24 p. 2741 - 2742
反应条件
1: 1.) Bu2SnO / 1.) MeOH, reflux, 3 h, 2.) dioxane, from 5 deg C to 10 deg C, 1 h
2: 73 percent / pyridine
View Scheme
参考文献
Tsuda, Yoshisuke; Sato, Yoshiyuki; Kanemitsu, Kimihiro; Hosoi, Shinzo; Shibayama, Kenji; Nakao, Kayo; Ishikawa, Yuko
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1465 - 1475
反应条件
1: 76 percent / tetrahydrofuran / 2 h / Heating
2: 71 percent / Bu3SnH; AIBN / dioxane; toluene / 2 h / Heating
View Scheme
参考文献
Tsui, Hon-Chung; Paquette, Leo A.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9968 - 9977
反应条件
1H-imidazole; iodine; triphenylphosphine in toluene
4 h; Heating;
参考文献
Mereyala, Hari Babu; Goud, P. Mallikarjun; Gadikota, Rajendrakumar Reddy; Reddy, K. Ramasubba
Journal of Carbohydrate Chemistry, 2000 , vol. 19, # 9 p. 1211 - 1222
反应条件
1: pyridine; chloroform; chlorocarbonic acid methyl ester
2: pyridine
View Scheme
参考文献
Reist et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1958,1961
