1,2-O-异亚丙基-D-呋喃葡萄糖合成路线 (共 73 条)
反应条件
(PhSO2)2; water in dichloromethane T=80°C;
参考文献
Markovic, Dean; Vogel, Pierre
Organic Letters, 2004 , vol. 6, # 16 p. 2693 - 2696
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in water; acetonitrile T=20°C; 4 h; selective removal of acetal group; other acetals and thioacetals of carbohydrates;
参考文献
Silva, Sandrina; Sanchez-Fernandez, Elena M.; Ortiz Mellet, Carmen; Tatibouet, Arnaud; Pilar Rauter, Amelia; Rollin, Patrick
European Journal of Organic Chemistry, 2013 , # 35 p. 7941 - 7951
反应条件
antimony trichloride in water; acetonitrile T=20°C; 0.333333 h;
参考文献
Wu, Qinpei; Wang, Yuan; Chen, Wei; Liu, Hua
Synthetic Communications, 2006 , vol. 36, # 10 p. 1361 - 1366
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in methanol 5 h; Ambient temperature;
参考文献
Baptistella, Lucia Helena B.; Santos, Jose Fernando dos; Ballabio, Karin Cristina; Marsaioli, Anita Jocelyne
Synthesis, 1989 , # 6 p. 436 - 438
反应条件
trifluoroacetic acid in dichloromethane Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 40, # 15 p. 2883 - 2886
反应条件
Propylene glycol; toluene-4-sulfonic acid in dichloromethane 1 h;
参考文献
Andrews, Mark A.; Gould, George L.
Carbohydrate Research, 1992 , vol. 229, # 1 p. 141 - 148
反应条件
osmium(VIII) oxide; 4-methylmorpholine N-oxide in water; acetone Ambient temperature;
参考文献
Carbohydrate Research, , vol. 179, p. 21 - 30
反应条件
hydrogenchloride in ethanol T=20°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 311, # 1-2 p. 89 - 94
反应条件
1: 71 percent / aq. H2SO4 / methanol; CH2Cl2 / 50 °C 2: 61 percent / (PhSO2)2; H2O / CH2Cl2 / 80 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 16 p. 2693 - 2696
反应条件
1: 93 percent / (PhSO2)2; H2O / CH2Cl2 / 80 °C 2: 92 percent / NaH; Bu4NI / tetrahydrofuran 3: 71 percent / aq. H2SO4 / methanol; CH2Cl2 / 50 °C 4: 61 percent / (PhSO2)2; H2O / CH2Cl2 / 80 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 16 p. 2693 - 2696