N-[2-(氨基羰基)苯基]-苯甲酰胺合成路线 （共 16 条）
反应条件
1: 65 percent / aq. H2O2; NaOEt 2: POCl3 / 100 °C View Scheme
参考文献
Purandare, Ashok V.; Gao, Aiming; Wan, Honghe; Somerville, John; Burke, Christine; Seachord, Carrie; Vaccaro, Wayne; Wityak, John; Poss, Michael A.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 10 p. 2669 - 2672
反应条件
T=218°C; Cyclization; 1 h;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 38, # 8 p. 905 - 908
反应条件
ammonium hydroxide
T=20°C;
参考文献
Chandrika, P. Mani; Yakaiah; Rao, A. Raghu Ram; Narsaiah; Reddy, N. Chakra; Sridhar; Rao, J. Venkateshwara
European Journal of Medicinal Chemistry, 2008 , vol. 43, # 4 p. 846 - 852
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane
参考文献
Purandare, Ashok V.; Gao, Aiming; Wan, Honghe; Somerville, John; Burke, Christine; Seachord, Carrie; Vaccaro, Wayne; Wityak, John; Poss, Michael A.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 10 p. 2669 - 2672
参考文献
Koerner
Journal fuer Praktische Chemie (Leipzig), 1887 , vol. <2> 36, p. 165
反应条件
palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; di-(1-adamantyl)-n-butylphosphine in N,N-dimethyl-formamide
T=100°C; P=7500.75 Torr; 16 h; Inert atmosphereAutoclave;
参考文献
Wu, Xiao-Feng; He, Lin; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2013 , vol. 19, # 38 p. 12635 - 12638
反应条件
tert.-butylhydroperoxide; zinc(II) iodide in water; dimethyl sulfoxide
T=80°C; 16 h;
参考文献
Sharif, Muhammad; Opalach, Julita; Langer, Peter; Beller, Matthias; Wu, Xiao-Feng
RSC Advances, 2014 , vol. 4, # 1 p. 8 - 17
参考文献
Alessandri
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1913 , vol. <5> 22 II, p. 231
反应条件
1: 84 percent / Et3N / acetone / 1 h / Heating
2: 6 percent / ammonium acetate; acetic acid / 1-methyl-pyrrolidin-2-one / 1 h / microwave heating
View Scheme
参考文献
Hradil, Pavel; Grepl, Martin; Hlavac, Jan; Lycka, Antonin
Heterocycles, 2007 , vol. 71, # 2 p. 269 - 280
反应条件
1: 84 percent / Et3N / acetone / 1 h / Heating
2: 6 percent / ammonium acetate; acetic acid / 1-methyl-pyrrolidin-2-one / 1 h / microwave heating
View Scheme
参考文献
Hradil, Pavel; Grepl, Martin; Hlavac, Jan; Lycka, Antonin
Heterocycles, 2007 , vol. 71, # 2 p. 269 - 280
