FMOC-L-3-(2-吡啶基)-丙氨酸合成路线 （共 5 条）
反应条件
lithium hydroxide in tetrahydrofuran T=20°C;
参考文献
Tabanella, Stefania; Valancogne, Ingrid; Jackson, Richard F W
Organic and biomolecular chemistry, 2003 , vol. 1, # 23 p. 4254 - 4261
反应条件
1.1: Zn; 1,2-dibromoethane; Me3SiCl / dimethylformamide / 2 h / 35 °C 1.2: 57 percent / Pd(PPh3)2Cl2 / dimethylformamide 2.1: 60 percent / aq. LiOH / tetrahydrofuran / 20 °C View Scheme
参考文献
Organic and biomolecular chemistry, , vol. 1, # 23 p. 4254 - 4261
反应条件
1.1: 94 percent / pyridine 2.1: 92 percent / NaI / acetone / 20 °C 3.1: Zn; 1,2-dibromoethane; Me3SiCl / dimethylformamide / 2 h / 35 °C 3.2: 57 percent / Pd(PPh3)2Cl2 / dimethylformamide 4.1: 60 percent / aq. LiOH / tetrahydrofuran / 20 °C View Scheme
参考文献
Organic and biomolecular chemistry, , vol. 1, # 23 p. 4254 - 4261
反应条件
1.1: Zn; 1,2-dibromoethane; Me3SiCl / dimethylformamide / 2 h / 35 °C 1.2: 57 percent / Pd(PPh3)2Cl2 / dimethylformamide 2.1: 60 percent / aq. LiOH / tetrahydrofuran / 20 °C View Scheme
参考文献
Organic and biomolecular chemistry, , vol. 1, # 23 p. 4254 - 4261
反应条件
1.1: 92 percent / NaI / acetone / 20 °C 2.1: Zn; 1,2-dibromoethane; Me3SiCl / dimethylformamide / 2 h / 35 °C 2.2: 57 percent / Pd(PPh3)2Cl2 / dimethylformamide 3.1: 60 percent / aq. LiOH / tetrahydrofuran / 20 °C View Scheme
参考文献
Organic and biomolecular chemistry, , vol. 1, # 23 p. 4254 - 4261
