1,1’-联萘-2,2’-二甲酸合成路线 （共 6 条）
反应条件
1: 127 mg / LiAlH4 / diethyl ether / 4 h / Heating 2: benzene; pyridine / room temp., overnight, reflux, 3 h 3: 42 percent / copper powder / dimethylformamide 4: 73 percent / KOH / aq. ethanol View Scheme
参考文献
Miyano, Sotaro; Handa, Shigeru; Shimizu, Kunitoshi; Tagami, Katsuya; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 7 p. 1943 - 1947
反应条件
lithium aluminium tetrahydride in diethyl ether 4 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 7 p. 1943 - 1947
反应条件
silver carbonate in acetone
T=40°C; 12 h;
参考文献
Furuta, Takumi; Nikaido, Masanori; Yamamoto, Junya; Kuribayashi, Toshifumi; Kawabata, Takeo
Synthesis (Germany), 2013 , vol. 45, # 10 art. no. SS-2013-F0057-OP, p. 1312 - 1318
反应条件
1: With acetic anhydride
0.75 h; Reflux;
2: T=280°C; 3 h; Inert atmosphere;
参考文献
Mala'Bi, Tahani; Pogodin, Sergey; Cohen, Shmuel; Agranat, Israel
RSC Advances, 2013 , vol. 3, # 44 p. 21797 - 21810
反应条件
sulfuric acid
T=100°C;
参考文献
Kalb
Chemische Berichte, 1914 , vol. 47, p. 1729
反应条件
nachfolgend Einw. von Aluminiumchlorid in Nitrobenzol;
参考文献
BASF; s. Kalb
Chemische Berichte, 1914 , vol. 47, p. 1729
