2,4,4-三甲氧基查尔酮合成路线 (共 2 条)
反应条件
sodium hydroxide in ethanol T=0 - 20°C; Claisen-Schmidt condensation;
参考文献
Bandgar, Babasaheb P.; Gawande, Shrikant S.; Bodade, Ragini G.; Totre, Jalinder V.; Khobragade, Chandrahas N.
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 3 p. 1364 - 1370
反应条件
4-tolylthallium(III) bis(trifluoroacetate); titanium tetrachloride 1.) benzene, RT, 30 min, 2.) THF, -78 deg C, 1.5 h, RT, 1 h; Yield given. Multistep reaction;
参考文献
Moriarty, Robert M.; Penmasta, Raju; Prakash, Indra; Awasthi, Alok K.
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 1022 - 1025