1-甲基-2-苯咪唑啉酮合成路线 (共 40 条)
反应条件
in dichloromethane 3 h; Heating;
参考文献
Li, Qun; Li, Tongmei; Woods, Keith W.; Gu, Wen-Zhen; Cohen, Jerry; Stoll, Vincent S.; Galicia, Tomas; Hutchins, Charles; Frost, David; Rosenberg, Saul H.; Sham, Hing L.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 11 p. 2918 - 2922
反应条件
N-methyl-pyrrolidine; selenium in tetrahydrofuran 1.) 31 kg/cm2, 100 degC, 20 h, 2.) 25 degC, 1 h;
参考文献
Yoshida, Tohru; Kambe, Nobuaki; Ogawa, Akiya; Sonoda, Noboru
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 137 - 148
反应条件
[DBU][HOAc] in neat (no solvent) T=120°C; P=67506.8 Torr; 24 h;
参考文献
Yu, Bo; Zhang, Hongye; Zhao, Yanfei; Chen, Sha; Xu, Jilei; Hao, Leiduan; Liu, Zhimin
ACS Catalysis, 2013 , vol. 3, # 9 p. 2076 - 2082
反应条件
hydrogen; palladium on activated charcoal in ethanol P=2585.7 Torr;
参考文献
Romero, Arthur G.; Darlington, William H.; Jacobsen, E. Jon; Mickelson, John W.
Tetrahedron Letters, 1996 , vol. 37, # 14 p. 2361 - 2364
反应条件
potassium tert-butylate; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane T=80°C; 18 h;
参考文献
Benedi, Carolina; Bravo, Fernando; Uriz, Pedro; Fernandez, Elena; Claver, Carmen; Castillon, Sergio
Tetrahedron Letters, 2003 , vol. 44, # 32 p. 6073 - 6077
反应条件
hydrogenchloride in water T=60°C; 1 h;
参考文献
Vernin, Gaston; Domlog, Hicham; Siv, Chan; Metzger, Jaques; El-Shafei, Ahmed Kamal
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 85 - 89
反应条件
caesium carbonate in water; N,N-dimethyl-formamide
参考文献
Merck and Co., Inc.
Patent: US5391566 A1, 1995 ;
US 5391566 A
反应条件
potassium hydroxide; [bis(acetoxy)iodo]benzene in methanol T=0°C; 1 h;
参考文献
Prakash; Batra; Kaur; Sharma; Singh; Moriarty
Synthesis, 2001 , # 4 p. 541 - 543
反应条件
hydrogen; 20percent Pd(OH)2/C in ethanol T=20°C; 24 h;
参考文献
Nakamura, Seikou; Tsuno, Naoki; Yamashita, Masayuki; Kawasaki, Ikuo; Ohta, Shunsaku; Ohishi, Yoshitaka
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 4 p. 429 - 436
反应条件
selenium; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine in toluene T=150°C; P=22800 Torr; 4 h;
参考文献
Wang, Xiaofang; Ling, Gang; Xue, Yan; Lu, Shiwei
European Journal of Organic Chemistry, 2005 , # 8 p. 1675 - 1679