3,4-二氯-5-氰基并噻唑合成路线 (共 8 条)
反应条件
disulfur dichloride in N,N-dimethyl-formamide T=100°C; 6 h;
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: EP2426114 A1, 2012 ;
Location in patent: Page/Page column 11 ;
反应条件
disulfur dichloride in N,N-dimethyl-formamide T=100°C; 3 h;
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: EP2426114 A1, 2012 ;
Location in patent: Page/Page column 12 ;
反应条件
disulfur dichloride in N,N-dimethyl-formamide T=100°C; 6 h;
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: EP2426114 A1, 2012 ;
Location in patent: Page/Page column 12 ;
反应条件
disulfur dichloride in N,N-dimethyl-formamide T=100°C; 3 h;
参考文献
IHARA CHEMICAL INDUSTRY CO., LTD.
Patent: US2012/46473 A1, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
1: in N,N-dimethyl-formamide T=60°C; 3 h; Inert atmosphere; 2: With chlorine in N,N-dimethyl-formamide T=60°C; 1 h; Inert atmosphere;
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: EP2426114 A1, 2012 ;
Location in patent: Page/Page column 13 ;
反应条件
1: With chlorine T=120°C; 16 h; 2: With disulfur dichloride in N,N-dimethyl-formamide T=100°C; 9 h; Product distribution / selectivity;
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: EP2426114 A1, 2012 ;
Location in patent: Page/Page column 12 ;
反应条件
disulfur dichloride in 1-methyl-pyrrolidin-2-one T=100°C; 6 h; Product distribution / selectivity;
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: EP2426114 A1, 2012 ;
Location in patent: Page/Page column 11 ;
反应条件
hydrogenchloride; sodium hydroxide
参考文献
Mitsui Toatsu Chemicals, Incorporated
Patent: US5240951 A1, 1993 ;