1: dimethyl malonate With n-butyllithium in diethyl ether
T=-78 - -10°C;
2: dodecanoyl chloride in diethyl ether
T=-10°C; 0.5 h;
参考文献
Geske, Grant D.; Wezeman, Rachel J.; Siegel, Adam P.; Blackwell, Helen E.
Journal of the American Chemical Society, 2005 , vol. 127, # 37 p. 12762 - 12763
1: dimethyl malonate With n-butyllithium in diethyl ether
T=-78 - -10°C;
2: butyryl chloride in diethyl ether
T=-10°C; 0.5 h;
参考文献
Geske, Grant D.; Wezeman, Rachel J.; Siegel, Adam P.; Blackwell, Helen E.
Journal of the American Chemical Society, 2005 , vol. 127, # 37 p. 12762 - 12763
