(1S,2S,5S)-(-)-2-羟基-3-蒎酮合成路线 （共 16 条）
反应条件
potassium permanganate; water in acetone T=-10 - -5°C; 20 h; Inert atmosphere;
参考文献
Hobuss, Dennis; Hasenjaeger, Jens; Driessen-Hoelscher, Birgit; Baro, Angelika; Axenov, Kirill V.; Laschat, Sabine; Frey, Wolfgang
Inorganica Chimica Acta, 2011 , vol. 374, # 1 p. 94 - 103
反应条件
triethylamine in dichloromethane; methylsulphoxide
反应条件
RuO4 in water; acetone T=-70°C; 0.0833333 h;
参考文献
Journal of Chemical Research, Miniprint, , # 9 p. 2442 - 2456
反应条件
3-chloro-benzenecarboperoxoic acid in water T=80°C; 3 h;
参考文献
Tetrahedron, , vol. 48, # 10 p. 1927 - 1942
反应条件
3-chloro-benzenecarboperoxoic acid in water T=80°C; 3 h;
参考文献
Thomas; Rey
Tetrahedron, 1992 , vol. 48, # 10 p. 1927 - 1942
反应条件
3-chloro-benzenecarboperoxoic acid in water T=80°C; 3 h;
参考文献
Tetrahedron, , vol. 48, # 10 p. 1927 - 1942
反应条件
potassium permanganate in water; acetone T=-10°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 51, # 30 p. 8363 - 8370
反应条件
potassium permanganate in water; acetone T=-10°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 51, # 30 p. 8363 - 8370
反应条件
sodium methylate in methanol T=25°C; 2 h; chromatographed on silica gel column using 3-5 percent ethyl acetate in hexane;
参考文献
Xenobiotica, , vol. 32, # 4 p. 251 - 265
反应条件
1: LDA / tetrahydrofuran / -80 deg C, 4 h; -80 deg C to rt, 24 h 2: 98 percent / 15percent citric acid / tetrahydrofuran / 96 h / Ambient temperature View Scheme
参考文献
Synlett, , vol. 1997, # 6 p. 691 - 692
