4-氯-(N-Boc)苯胺合成路线 (共 35 条)
反应条件
Cu(BF4)2 T=30 - 33°C; 0.5 h;
参考文献
Chankeshwara, Sunay V.; Chakraborti, Asit K.
Tetrahedron Letters, 2006 , vol. 47, # 7 p. 1087 - 1091
反应条件
cBRIDP; bis(η3-allyl-μ-chloropalladium(II)); tri-iso-propylsilanol; potassium hydroxide in water T=50°C; 20 h; Inert atmosphereGreen chemistry;
参考文献
Isley, Nicholas A.; Dobarco, Sebastian; Lipshutz, Bruce H.
Green Chemistry, 2014 , vol. 16, # 3 p. 1480 - 1488
反应条件
ammonium hydroxide; iron in methanol T=25°C; Reduction; condensation; 1 h; sonication;
参考文献
Chandrasekhar; Narsihmulu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7969 - 7972
反应条件
lead(IV) acetate in tetrachloromethane 0.666667 h; Heating;
参考文献
Leardini, Rino; Zanardi, Giuseppe
Synthesis, 1982 , # 3 p. 225 - 227
反应条件
T=20°C; 2 h; Heating / reflux;
参考文献
WO2003/106452 A2, ;
Page 148-149 ;
WO 03/106452 A2
反应条件
lead(IV) acetate; triethylamine
参考文献
Journal of the American Chemical Society, , vol. 87, p. 1141 - 1142
反应条件
di-tert-butyl peroxide in chlorobenzene T=110°C; 48 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 3164 - 3167
反应条件
di-tert-butyl peroxide in chlorobenzene T=110°C; 48 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 3164 - 3167
反应条件
di-tert-butyl peroxide in chlorobenzene T=110°C; 48 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 3164 - 3167
反应条件
1: bis-[(trifluoroacetoxy)iodo]benzene / 1,2-dichloro-ethane / 0.03 h / |Molecular sieve; |Inert atmosphere 2: 1,2-dichloro-ethane / 1 h / 60 °C / |Molecular sieve; |Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 14 p. 2172 - 2175