4-硝基苯基氨基甲酸叔丁酯合成路线 （共 23 条）
反应条件
in dichloromethane Reflux;
参考文献
Uno, Masaharu; Ban, Hyun Seung; Nabeyama, Wataru; Nakamura, Hiroyuki
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 6 p. 979 - 981
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Uno, Masaharu; Ban, Hyun Seung; Nakamura, Hiroyuki
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 12 p. 3166 - 3169
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in N,N-dimethyl-formamide T=80°C; 24 h; Inert atmosphere;
参考文献
Jones, Kerri L.; Porzelle, Achim; Hall, Adrian; Woodrow, Michael D.; Tomkinson, Nicholas C. O.
Organic Letters, 2008 , vol. 10, # 5 p. 797 - 800
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=100°C; 2.5 h;
参考文献
Qin, Lijin; Cui, Hongmeng; Zou, Dapeng; Li, Jingya; Wu, Yangjie; Zhu, Zhiwu; Wu, Yusheng
Tetrahedron Letters, 2010 , vol. 51, # 33 p. 4445 - 4448
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=100°C; 1.5 h;
参考文献
Qin, Lijin; Cui, Hongmeng; Zou, Dapeng; Li, Jingya; Wu, Yangjie; Zhu, Zhiwu; Wu, Yusheng
Tetrahedron Letters, 2010 , vol. 51, # 33 p. 4445 - 4448
反应条件
1: 4-nitro-benzoyl chloride With pyridine; trimethylsilylazide in N,N-dimethyl-formamide T=20°C; Curtius rearrangement; Microflow reactionInert atmosphere; 2: tert-butyl alcohol With acetic acid in N,N-dimethyl-formamide T=110°C; Microflow reactionInert atmosphere;
参考文献
Ishikawa, Hayato; Bondzic, Bojan P.; Hayashi, Yujiro
European Journal of Organic Chemistry, 2011 , # 30 p. 6020 - 6031
反应条件
silver carbonate in ethylene glycol dimethyl ether T=80°C; 48 h;
参考文献
Lee, Kang-Sang; Lim, Young-Kwan; Cho, Cheon-Gyu
Tetrahedron Letters, 2002 , vol. 43, # 42 p. 7463 - 7464
反应条件
nitric acid; acetic anhydride T=20°C; 1.5 h; Cooling with ice;
参考文献
Tetrahedron Letters, , vol. 53, # 32 p. 4154 - 4155
反应条件
1: 5-chloro-2-nitro-phenylamine With sodium hydride in tetrahydrofuran T=0 - 20°C; 0.666667 h; 2: di-tert-butyl dicarbonate in tetrahydrofuran T=20°C; 2 h; 3: methyl iodide in tetrahydrofuran T=60°C; 10 h;
参考文献
Sumitomo Chemical Company, Limited
Patent: EP1172356 A1, 2002 ;
Location in patent: Page 8 ;
反应条件
1: 2-nitro-aniline With sodium hydride in tetrahydrofuran T=0 - 20°C; 0.666667 h; 2: di-tert-butyl dicarbonate in tetrahydrofuran T=20°C; 2 h; 3: dimethyl sulfate in tetrahydrofuran T=20°C; 2 h;
参考文献
Sumitomo Chemical Company, Limited
Patent: EP1172356 A1, 2002 ;
Location in patent: Page 8 ;
反应条件
lead(IV) acetate in tetrachloromethane 0.333333 h; Heating;
参考文献
Leardini, Rino; Zanardi, Giuseppe
Synthesis, 1982 , # 3 p. 225 - 227
