1.1: 96 percent / 1 h / 90 °C
2.1: 31 percent / diphenyl ether / 0.5 h / 255 °C
3.1: 64 percent / 10 percent aq. NaOH / 0.5 h / 100 °C
4.1: NH4OH; AgNO3 / H2O / 0.5 h / Heating
4.2: 34 percent / diphenyl ether / 1 h / 255 °C
5.1: 98 percent / phosphorus oxychloride / 0.75 h / 110 °C
View Scheme
参考文献
Vippagunta, Sudha Rani; Dorn, Arnulf; Matile, Hugues; Bhattacharjee, Apurba K.; Karle, Jean M.; Ellis, William Y.; Ridley, Robert G.; Vennerstrom, Jonathan L.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 22 p. 4630 - 4639
1.1: 31 percent / diphenyl ether / 0.5 h / 255 °C
2.1: 64 percent / 10 percent aq. NaOH / 0.5 h / 100 °C
3.1: NH4OH; AgNO3 / H2O / 0.5 h / Heating
3.2: 34 percent / diphenyl ether / 1 h / 255 °C
4.1: 98 percent / phosphorus oxychloride / 0.75 h / 110 °C
View Scheme
参考文献
Vippagunta, Sudha Rani; Dorn, Arnulf; Matile, Hugues; Bhattacharjee, Apurba K.; Karle, Jean M.; Ellis, William Y.; Ridley, Robert G.; Vennerstrom, Jonathan L.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 22 p. 4630 - 4639
1.1: NH4OH; AgNO3 / H2O / 0.5 h / Heating
1.2: 34 percent / diphenyl ether / 1 h / 255 °C
2.1: 98 percent / phosphorus oxychloride / 0.75 h / 110 °C
View Scheme
参考文献
Vippagunta, Sudha Rani; Dorn, Arnulf; Matile, Hugues; Bhattacharjee, Apurba K.; Karle, Jean M.; Ellis, William Y.; Ridley, Robert G.; Vennerstrom, Jonathan L.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 22 p. 4630 - 4639
1.1: 64 percent / 10 percent aq. NaOH / 0.5 h / 100 °C
2.1: NH4OH; AgNO3 / H2O / 0.5 h / Heating
2.2: 34 percent / diphenyl ether / 1 h / 255 °C
3.1: 98 percent / phosphorus oxychloride / 0.75 h / 110 °C
View Scheme
参考文献
Vippagunta, Sudha Rani; Dorn, Arnulf; Matile, Hugues; Bhattacharjee, Apurba K.; Karle, Jean M.; Ellis, William Y.; Ridley, Robert G.; Vennerstrom, Jonathan L.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 22 p. 4630 - 4639
