3,6,9,12,15,18-六氧杂十九烷-1-胺合成路线 （共 5 条）
反应条件
hydrogenchloride; potassium hydroxide; hydrazine in ethanol; chloroform
参考文献
Competitive Technologies, Inc.
Patent: US5606038 A1, 1997 ;
反应条件
hydrogen; palladium on activated charcoal in methanol P=5250.4 Torr; 4 h;
参考文献
Seguer, J.; Selve, C.; Allouch, M.; Infante, M. R.
Journal of the American Oil Chemists' Society, 1996 , vol. 73, # 1 p. 79 - 86
反应条件
1: Et3N / CH2Cl2 / -10 - 20 °C 2: NaN3, tetrabutylammonium hydrogen sulfate / dimethylformamide / 5 h / 40 °C 3: 61 percent / H2 / Pd/C / methanol / 4 h / 5250.4 Torr View Scheme
参考文献
Journal of the American Oil Chemists' Society, , vol. 73, # 1 p. 79 - 86
反应条件
1: NaN3, tetrabutylammonium hydrogen sulfate / dimethylformamide / 5 h / 40 °C 2: 61 percent / H2 / Pd/C / methanol / 4 h / 5250.4 Torr View Scheme
参考文献
Journal of the American Oil Chemists' Society, , vol. 73, # 1 p. 79 - 86
反应条件
1: 39 percent / NaH / tetrahydrofuran / 5 h / Heating 2: 68 percent / triethylamine / tetrahydrofuran / 24 h / Ambient temperature 3: dimethylformamide / 3 h / 120 °C 4: hydrazine / ethanol / 1.5 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 117, # 23 p. 6249 - 6253
