N-苯基-1,3-苯并噻唑-2-胺合成路线 (共 75 条)
反应条件
sulfur
T=220 - 300°C; P=45004.5 - 83258.3 Torr; Product distribution / selectivity;
参考文献
DUSLO A.S.
Patent: WO2005/61471 A1, 2005 ;
Location in patent: Page/Page column 8-9; 9-10 ;
反应条件
1,1'-(ethane-1,2-diyl)dipyridinium ditribromide; triethylamine in acetonitrile
T=20°C;
参考文献
Yella, Ramesh; Patel, Bhisma K.
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 5 p. 754 - 763
反应条件
potassium carbonate in water
T=100°C; 33 h; Green chemistry;
参考文献
Rout, Saroj Kumar; Guin, Srimanta; Nath, Jayashree; Patel, Bhisma K.
Green Chemistry, 2012 , vol. 14, # 9 p. 2491 - 2498
反应条件
potassium carbonate in water
T=100°C; 43 h; Green chemistry;
参考文献
Rout, Saroj Kumar; Guin, Srimanta; Nath, Jayashree; Patel, Bhisma K.
Green Chemistry, 2012 , vol. 14, # 9 p. 2491 - 2498
反应条件
1: acetic acid
2: Et3N / acetone / Heating
3: NaOH / Ambient temperature
4: aq. HCl
5: aq. HCl
6: CH2Cl2 / Heating
View Scheme
参考文献
Takahashi,S. et al.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 1176 - 1184
反应条件
1: Et3N / acetone / Heating
2: NaOH / Ambient temperature
3: aq. HCl
4: aq. HCl
5: CH2Cl2 / Heating
View Scheme
参考文献
Takahashi,S. et al.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 1176 - 1184
反应条件
1: NaNH2, isopentyl nitrite / liquid ammonia
2: acetic acid
3: Et3N / acetone / Heating
4: NaOH / Ambient temperature
5: aq. HCl
6: aq. HCl
7: CH2Cl2 / Heating
View Scheme
参考文献
Takahashi,S. et al.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 1176 - 1184
反应条件
1: aq. HCl
2: CH2Cl2 / Heating
View Scheme
参考文献
Takahashi,S. et al.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 1176 - 1184
反应条件
1: NaOH / Ambient temperature
2: aq. HCl
3: aq. HCl
4: CH2Cl2 / Heating
View Scheme
参考文献
Takahashi,S. et al.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 1176 - 1184
反应条件
1: aq. HCl
2: aq. HCl
3: CH2Cl2 / Heating
View Scheme
参考文献
Takahashi,S. et al.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 1176 - 1184