1,2-bis-(diphenylphosphino)ethane; bis(dibenzylideneacetone)-palladium(0) in dimethyl sulfoxide
T=120°C; 12 h; Title compound not separated from byproducts.;
1: 1-phenylallyl benzoate With C48H50IrNO4P in tetrahydrofuran
T=0°C; 3 h; Inert atmosphere;
2: sodium salt of dimethylmalonate in tetrahydrofuran
T=0°C; 14 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Stanley, Levi M.; Bai, Chen; Ueda, Mitsuhiro; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 26 p. 8918 - 8920
