(2,2-二甲基-1,3-二氧戊环-4-基)甲基棕榈酸酯合成路线 (共 7 条)
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in benzene T=0 - 10°C; 1 h;
参考文献
Mori, Kenji
Tetrahedron, 2012 , vol. 68, # 40 p. 8441 - 8449
反应条件
1: 2,2-dimethyl-1,3-dioxolane-4-methanol With sodium ethanolate in ethanol 2: hexadecanoic acid methyl ester in ethanol T=20 - 100°C;
参考文献
Yakovleva; Shayakhmetova; Gumerov; Ishmuratov
Chemistry of Natural Compounds, 2004 , vol. 40, # 6 p. 593 - 594
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in diethyl ether T=20 - 25°C; Esterification; 4.5 h;
参考文献
Wang, Xiaosan; Wang, Xingguo; Jin, Qingzhe; Wang, Tong
JAOCS, Journal of the American Oil Chemists' Society, 2013 , vol. 90, # 10 p. 1455 - 1463
反应条件
immobilized Rhizomucor miehei lipase in n-heptane T=60°C; 4 h; Enzymatic reaction;
参考文献
Junior, Ivaldo I.; Flores, Marcela C.; Sutili, Felipe K.; Leite, Selma G.F.; De M. E Miranda, Leandro S.; Leal, Ivana C.R.; De Souza, Rodrigo O.M.A.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 77, p. 53 - 58
参考文献
Amberger; Wiesehahn
Z. Unters. Nahr.-Genussm., vol. 46, p. 298
Chem. Zentralbl., 1924 , vol. 95, # I p. 1879
反应条件
sodium carbonate T=125 - 140°C; 6 h; Neat (no solvent);
参考文献
Batista, Luciano N.; San Gil, Rosane A. S.; Lopes, Luciana B. R.; Soares, Vera L. P.
Journal of Thermal Analysis and Calorimetry, 2011 , vol. 106, # 3 p. 697 - 702
反应条件
hydrogenchloride; sodium sulfate
参考文献
Bergmann; Carter
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1930 , vol. 191, p. 211,220