5-(4-氯苯基)四氢呋喃-2(3H)-酮合成路线 (共 17 条)
反应条件
methanesulfonic acid; C21H12F9P*C8H18NO4S2(1-)*Au(1+); 3-chloro-benzenecarboperoxoic acid in 1,2-dichloro-ethane T=20°C; 5 h;
参考文献
Shu, Chao; Liu, Meng-Qi; Sun, Yu-Zhe; Ye, Long-Wu
Organic Letters, 2012 , vol. 14, # 18 p. 4958 - 4961,4
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Shu, Chao; Liu, Meng-Qi; Sun, Yu-Zhe; Ye, Long-Wu
Organic Letters, 2012 , vol. 14, # 18 p. 4958 - 4961
反应条件
sodium acetate; copper diacetate; Manganese (II) acetate in acetic anhydride; acetic acid T=95 - 97°C; anodic oxidation;
参考文献
Shundo, Ryushi; Nishiguchi, Ikuzo; Matsubara, Yoshiharu; Hirashima, Tsuneaki
Tetrahedron, 1991 , vol. 47, # 4/5 p. 831 - 840
反应条件
1: With titanium(IV) isopropylate; trimethylsilyl trifluoromethanesulfonate; (R)-2,2'-dihydroxy-1,1'-binaphthyl in chloroform-d1; acetonitrile-D3 T=0°C; 80 h; 2: With toluene-4-sulfonic acid in benzene Further stages.;
参考文献
Martins, Evelyn O.; Gleason, James L.
Organic Letters, 1999 , vol. 1, # 10 p. 1643 - 1645
反应条件
sodium tetrahydroborate; tetrabutylammomium bromide in benzene T=20 - 25°C; 1 h;
参考文献
Rao, C. Someswara; Deshmukh, A. A.; Patel, B. J.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 626 - 629
反应条件
oxygen; sodium acetate; copper(II) bis(trifluoromethanesulfonate); lithium bromide T=120°C; P=760.051 Torr; 12 h;
参考文献
Huang, Liangbin; Jiang, Huanfeng; Qi, Chaorong; Liu, Xiaohang
Journal of the American Chemical Society, 2010 , vol. 132, # 50 p. 17652 - 17654
反应条件
samarium diiodide; ethanol in tetrahydrofuran 5 h; Heating;
参考文献
Bradley; Williams; Blann; Holzapfel
Synthetic Communications, 2001 , vol. 31, # 2 p. 203 - 209
反应条件
samarium diiodide; ethanol in tetrahydrofuran 5 h; Heating;
参考文献
Bradley; Williams; Blann; Holzapfel
Synthetic Communications, 2001 , vol. 31, # 2 p. 203 - 209
反应条件
1: diethyl ether / 1 h / -30 - 20 °C 2: C21H12F9P*C8H18NO4S2(1-)*Au(1+); 3-chloro-benzenecarboperoxoic acid; methanesulfonic acid / 1,2-dichloro-ethane / 5 h / 20 °C View Scheme
参考文献
Bradley; Williams; Blann; Holzapfel
Synthetic Communications, 2001 , vol. 31, # 2 p. 203 - 209
反应条件
ammonium cerium(IV) nitrate; nitric acid in acetonitrile 8 h; Heating;
参考文献
Nagarajan, A.; Porchezhiyan, V.; Srinivasaramanujam; Balasubramanian, T. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1202 - 1203
反应条件
dipotassium peroxodisulfate; potassium acetate; acetic acid ; ferriacetate T=123°C; 0.583333 h; various time of olefin addn.; Product distribution;
参考文献
Giordano, Claudio; Belli, Aldo; Casagrande, Francesco; Guglielmetti, Gianfranco; Citterio, Atillio
Journal of Organic Chemistry, 1981 , vol. 46, # 15 p. 3149 - 3151