1,4-二氧杂螺[4.6]十一烷合成路线 (共 11 条)
反应条件
toluene-4-sulfonic acid 0.0333333 h; Irradiation;
参考文献
Moghaddam; Sharifi
Synthetic Communications, 1995 , vol. 25, # 16 p. 2457 - 2461
反应条件
boron trifluoride diethyl etherate in dichloromethane 1.16667 h; Ambient temperature;
参考文献
Torok, Daniel S.; Figueroa, John J.; Scott, William J.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7274 - 7276
反应条件
EM-3993 in acetonitrile Irradiation;
参考文献
Gassman, Paul G.; Burns, Stephen J.
Journal of Organic Chemistry, 1988 , vol. 53, # 23 p. 5576 - 5578
反应条件
T=25°C; 15 h; Irradiation;
参考文献
Kropp, Paul J.; McNeely, Steven A.; Davis, Robert Drummond
Journal of the American Chemical Society, 1983 , vol. 105, # 23 p. 6907 - 6915
反应条件
T=25°C; 12 h; Irradiation;
参考文献
Kropp, Paul J.; McNeely, Steven A.; Davis, Robert Drummond
Journal of the American Chemical Society, 1983 , vol. 105, # 23 p. 6907 - 6915
参考文献
Sonawane, H. R.; Nanjundiah, B. S.; Panse, M. D.
Tetrahedron Letters, 1985 , vol. 26, # 29 p. 3507 - 3510
反应条件
Product distribution;
参考文献
Bauduin, G.; Bondon, D.; Pietrasanta, Y.; Pucci, B.
Tetrahedron, 1980 , vol. 36, # 2 p. 245 - 254
反应条件
ammonium cerium(IV) nitrate in methanol; water T=20°C; Ring cleavage; 0.166667 h;
参考文献
Nair, Vijay; Nair, Latha G.; Balagopal, Lakshmi; Rajan, Roshini
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999 , vol. 38, # 11 p. 1234 - 1236
反应条件
1: 1.) Te, NaBH4, 2.) H2O / 1.) EtOH, 25 deg C, 30 min 2: 81 percent / conc. H2SO4 / methanol; H2O / 25 °C View Scheme
参考文献
Lue, Ping; Fan, Wei-Qiang; Zhou, Xun-Jun
Synthesis, 1989 , # 9 p. 692 - 693
反应条件
(i) Br2, MeOH, (ii) /BRN= 3592982/, DMSO; Multistep reaction;
参考文献
Garbisch,E.W.
Journal of Organic Chemistry, 1965 , vol. 30, # 7 p. 2109 - 2120