6-甲氧基-alpha-苯并吡喃合成路线 （共 9 条）
反应条件
Au(Ph3P)+NTf2- in dichloromethane T=25°C; 0.25 h; regioselective reaction;
参考文献
Lykakis, Ioannis N.; Efe, Christina; Gryparis, Charis; Stratakis, Manolis
European Journal of Organic Chemistry, 2011 , # 12 p. 2334 - 2338
反应条件
air; water; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0) in dimethyl sulfoxide T=60°C; 72 h;
参考文献
Larock, Richard C.; Wei, Lulin; Hightower, Timothy R.
Synlett, 1998 , # 5 p. 522 - 524
反应条件
ClAu(di(tert-butyl)(1,1′-biphenyl-2-yl)-phosphine); silver trifluoromethanesulfonate in tetrahydrofuran T=65°C; 20 h; Inert atmosphere;
参考文献
Aponick, Aaron; Biannic, Berenger; Jong, Michael R.
Chemical Communications, 2010 , vol. 46, # 36 p. 6849 - 6851
反应条件
1: With 9-bora-bicyclo[3.3.1]nonane in tetrahydrofuran T=20°C; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water T=20°C; 6 h;
参考文献
Eguchi; Hoshino
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 5 p. 967 - 970
反应条件
in 1,2-dichloro-ethane T=70°C; 3 h;
参考文献
Efe, Christina; Lykakis, Ioannis N.; Stratakis, Manolis
Chemical Communications, 2011 , vol. 47, # 2 p. 803 - 805
反应条件
toluene-4-sulfonic acid in benzene 72 h; Heating;
参考文献
Schuda, Paul Francis; Phillips, Jennifer L.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 669 - 672
反应条件
1: 1.) potassium hydride; 2.) tetra-n-butylammonium iodide / 1.) THF, room temp., 15 min; 2.) reflux, 4 d 2: 26 percent / p-toluenesulfonic acid / benzene / 72 h / Heating View Scheme
参考文献
Lykakis, Ioannis N.; Efe, Christina; Gryparis, Charis; Stratakis, Manolis
European Journal of Organic Chemistry, 2011 , # 12 p. 2334 - 2338
反应条件
1: caesium carbonate / N,N-dimethyl-formamide / 20 °C 2: / 1,2-dichloro-ethane / 3 h / 70 °C View Scheme
参考文献
Efe, Christina; Lykakis, Ioannis N.; Stratakis, Manolis
Chemical Communications, 2011 , vol. 47, # 2 p. 803 - 805
反应条件
1: H2 / 10 percent Pd-C / acetic acid / Ambient temperature 2: 47 percent (w/v) HBr / acetic acid / 100 - 110 °C View Scheme
参考文献
Shiratsuchi; Kawamura; Akashi; Fujii; Ishihama; Uchida
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 2 p. 632 - 641
