N-(6-甲氧基-3-吡啶基)氨基甲酸叔丁酯合成路线 （共 4 条）
反应条件
in 1,4-dioxane Reflux;
参考文献
SANOFI-AVENTIS
Patent: US2011/178053 A1, 2011 ;
Location in patent: Page/Page column 46 ;
US 20110178053 A1
反应条件
in methanol 15 h; Heating; Yield given;
参考文献
Hongo, Hiroshi; Nakano, Hiroto; Okuyama, Yuko
Heterocycles, 1995 , vol. 40, # 2 p. 831 - 836
反应条件
1: 67 percent / TMEDA, BuLi / diethyl ether; hexane / 1.) -40 deg C, 16 h, 2.) -40 deg C to r.t., 1 h 2: 93 percent / aq. KOH / 18 h / Heating View Scheme
参考文献
Rewcastle, Gordon W.; Denny, William A.; Winters, R. Thomas; Colbry, Norman L.; Showalter, H. D. Hollis
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2221 - 2226
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane 1.) -40 deg C, 16 h, 2.) -40 deg C to r.t., 1 h;
参考文献
Rewcastle, Gordon W.; Denny, William A.; Winters, R. Thomas; Colbry, Norman L.; Showalter, H. D. Hollis
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2221 - 2226
