反应条件
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 0 - 20 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 1.25 h / 0 - 20 °C
3.2: 20 °C
4.1: tetrabutyl ammonium fluoride / 24 h
View Scheme
参考文献
Han, Long; Liu, Chuan; Zhang, Wei; Shi, Xiao-Xin; You, Shu-Li
Chemical Communications, 2014 , vol. 50, # 10 p. 1231 - 1233
