sodium iodide in butanone 6 h; Heating;

diphosphorous tetraiodide in carbon disulfide 4 h; Ambient temperature;

diiodo monosilane in chloroform 1.25 h; Ambient temperature;

acetone; sodium iodide

acetone; sodium iodide

hydrogen iodide

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in tetrahydrofuran byproducts: NaI; under inert atmosphere, to suspn. of Co complex in THF added 1,3-diiodobutane, stirred for 2 h; hexane added, filtered, solvent removed under vac., residue chromd., solvent removed under vac., recrystd. from toluene/hexane, filtered, washed with cold pentane, dried under vac., elem. anal.;