1,3-双(4-氯苯基)-1,3-丙二酮合成路线 （共 17 条）
反应条件
iodine; dimethyl sulfoxide T=150°C; 27 h;
参考文献
Yuan, Yu; Zhu, Haitao
European Journal of Organic Chemistry, 2012 , # 2 p. 329 - 333
反应条件
formaldehyd; hydroxocobalt(III) Schiff base T=60°C; 0.7 h;
参考文献
Tetrahedron Letters, , vol. 36, # 31 p. 5609 - 5612
反应条件
methanol; hydroxocobalt(III) Schiff base T=60°C; 0.7 h;
参考文献
Tetrahedron Letters, , vol. 36, # 31 p. 5609 - 5612
反应条件
formaldehyd; hydroxocobalt(III) Schiff base T=60°C; 0.7 h;
参考文献
Tetrahedron Letters, , vol. 36, # 31 p. 5609 - 5612
反应条件
methanol; hydroxocobalt(III) Schiff base T=60°C; 0.7 h;
参考文献
Tetrahedron Letters, , vol. 36, # 31 p. 5609 - 5612
反应条件
1: 95 percent / TsN3, KF 2: 86 percent / Al2O3 / pentane; diethyl ether View Scheme
参考文献
Korneev; Richter
Synthesis, 1995 , # 10 p. 1248 - 1250
反应条件
potassium fluoride; 4-toluenesulfonyl azide
参考文献
Korneev; Richter
Synthesis, 1995 , # 10 p. 1248 - 1250
反应条件
1,3-dibenzyl-1H-benzo[d]imidazol-3-ium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
T=20°C; 0.283333 h; Inert atmosphere;
参考文献
Singh, Santosh; Singh, Pankaj; Rai, Vijai K.; Kapoor, Ritu; Yadav, Lal Dhar S.
Tetrahedron Letters, 2011 , vol. 52, # 1 p. 125 - 128
反应条件
1: para-chloroacetophenone With lithium hexamethyldisilazane in toluene
T=0°C;
2: 4-chlorobenzoic acid methyl ester in toluene
Further stages.;
参考文献
Dhondi, Pawan K.; Carberry, Patrick; Chisholm, John D.
Tetrahedron Letters, 2007 , vol. 48, # 49 p. 8743 - 8746
反应条件
hydrogenchloride; sodium methylate in tetrahydrofuran
参考文献
G.D. Searle and Co.
Patent: US5434178 A1, 1995 ;
