反应条件
in diethyl ether byproducts: LiF; under inert gas, at -78°C, warmed to room temp. stirred for 10 h at 20°C; filtered, solvent removed in vacuo, pentane added, cooled to -20°C, filtered, fractional crystd. (Et2O/pentane); elem. anal.;
参考文献
Lazraq, M.; Couret, C.; Escudie, J.; Satge, J.; Soufiaoui, M.
Polyhedron, 1991 , vol. 10, p. 1153 - 1162
