4-(甲氨基)苯甲酸甲酯合成路线 (共 26 条)
反应条件
in diethyl ether T=0 - 25°C; 0.416667 h;
参考文献
Synthesis, , # 5 p. 742 - 750
反应条件
hydrogenchloride; thionyl chloride in methanol 1.5 h; Heating;
参考文献
Kavalek, Jaromir; Kralikova, Ulrika; Machacek, Vladimir; Sedlak, Milos; Sterba, Vojeslav
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 1 p. 202 - 222
反应条件
1: 93 percent / pyridine / CH2Cl2 / 20 °C 2: 100 percent / CH2Cl2 / 0.17 h / 20 °C 3: 95 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 62, # 25 p. 6100 - 6106
反应条件
methanesulfonic acid; hydrogen; [Ru(acac)3]; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=140°C; 5 h; AutoclaveInert atmosphere;
参考文献
Li, Yuehui; Sorribes, Ivan; Yan, Tao; Junge, Kathrin; Beller, Matthias
Angewandte Chemie - International Edition, 2013 , vol. 52, # 46 p. 12156 - 12160
Angew. Chem., 2013 , vol. 125, # 46 p. 12378 - 12382,5
反应条件
sodium tetrahydroborate; palladium on activated charcoal 1) THF, 20 min, -78 deg C, 2) 20 deg C, 8 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 43, # 18 p. 4221 - 4226
反应条件
NaY faujasite in xylene T=135°C; 4.5 h; Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 70, # 7 p. 2476 - 2485
参考文献
Chemische Berichte, , vol. 51, p. 1043,1044
反应条件
phosphate buffer; water T=25°C; other reaction partner; Rate constantMechanism;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 55, # 1 p. 202 - 222
反应条件
acetate buffer T=25°C; other reaction partners; Rate constantMechanism;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 55, # 1 p. 202 - 222
反应条件
T=25°C; Rate constantMechanism;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 55, # 1 p. 202 - 222